carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester

Base Information

• Chemical Name: carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester
• CAS No.: 631901-97-8
• Molecular Formula: C₄₆H₆₄N₄O₁₃
• Molecular Weight: 881.033

Synonyms:carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester

Chemical Property of carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester

Chemical Property:

Purity/Quality:

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Technology Process of carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester

There total 2 articles about carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2E)-3-[4-(2-pyridazinyl)phenyl]-2-propen-1-ol (545420-91-5) + 1H-pyrrole-1-carboxylic acid, 3-cyano-, (3aS,4R,7R,BS,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl ester (631901-96-7) → carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester (631901-97-8)

Guidance literature:

(2E)-3-[4-(2-pyridazinyl)phenyl]-2-propen-1-ol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dimethyl sulfoxide; for 0.25h;

1H-pyrrole-1-carboxylic acid, 3-cyano-, (3aS,4R,7R,BS,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl ester; In tetrahydrofuran; dimethyl sulfoxide; for 5h;

With sodium hydrogencarbonate; In tetrahydrofuran; water; dimethyl sulfoxide; ethyl acetate;

Reference yield: 48.0%

(2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propen-1-ol (545420-82-4) + 1H-pyrrole-1-carboxylic acid, 3-cyano-, (3aS,4R,7R,BS,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl ester (631901-96-7) → carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester (631901-97-8)

Guidance literature:

(2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propen-1-ol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 0.0833333h;

1H-pyrrole-1-carboxylic acid, 3-cyano-, (3aS,4R,7R,BS,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl ester; In tetrahydrofuran; dimethyl sulfoxide; at 0 ℃; for 2h;

With sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;

Reference yield: 82.0%

carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester (631901-97-8) + pyridin-2-yl acetic acid hydrochloride (16179-97-8) → 2-pyridineacetic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-4-ethyltetradecahydro-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-11-[[[[(2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl]oxy]carbonyl]oxy]-10-[[3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-2H-oxacyclotetradecino[4,3-d]oxazol-8-yl ester

Guidance literature:

carbonic acid, (3aS,4R,7R,8S,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl (2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propenyl ester; pyridin-2-yl acetic acid hydrochloride; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In dichloromethane; at 20 ℃; for 16h;

With sodium hydrogencarbonate; In dichloromethane; water; ethyl acetate;

With methanol; at 20 ℃; for 20h;

upstream raw materials:

(2E)-3-[4-(2-pyrimidinyl)phenyl]-2-propen-1-ol

1H-pyrrole-1-carboxylic acid, 3-cyano-, (3aS,4R,7R,BS,9S,10R,11R,13R,15R,15aR)-10-[[2-O-acetyl-3,4,6-trideoxy-3-(dimethylamino)-β-D-xylo-hexopyranosyl]oxy]-4-ethyltetradecahydro-8-hydroxy-3a,7,9,11,13,15-hexamethyl-2,6,14-trioxo-2H-oxacyclotetradecino[4,3-d]oxazol-11-yl ester

(2E)-3-[4-(2-pyridazinyl)phenyl]-2-propen-1-ol

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