phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside
CAS No.:1352299-28-5
Molecular Formula:C₄₃H₄₁ClO₉S
Molecular Weight:769.312
Hs Code.:

Synonyms:phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: phenyl 2,3,-di-O-benzoyl-4-O-benzyl-1-thio-β-D-glucopyranoside

: 165274-92-0
4-<2-(2-Chloroethoxy)ethoxy>phenole

: 1352299-28-5
phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 60 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.030

Reference yield: 100.0%

: 1352299-28-5
phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

: 1352299-29-6
phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium azide; tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 30h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.030

Reference yield:

: 1352299-28-5
phenyl 2,3-O-di-benzoyl-4-O-benzyl-6-O-{4-[2-(2-chloroethoxy)ethoxy]phenyl}-1-thio-β-D-glucopyranoside

: C₄₃H₄₃NO₉S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 30 h / 60 °C / Inert atmosphere

2: ammonium chloride; zinc / tetrahydrofuran; water / 0.17 h / 0 - 20 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; ammonium chloride; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.030