2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

Base Information

Chemical Name:2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione
CAS No.:1192573-82-2
Molecular Formula:C₂₅H₁₉N₅O₃
Molecular Weight:437.458
Hs Code.:

Synonyms:2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

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Chemical Property of 2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

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Technology Process of 2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

There total 3 articles about 2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1192575-99-7
N-hydroxy-1-(1-methyl-1H-imidazol-5-yl)-1-phenylmethanimine

: 83592-42-1
2-(6-bromomethylpyridin-2-yl)isoindole-1,3-dione

: 1192573-82-2
2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

Guidance literature:: With caesium carbonate; potassium iodide; In acetonitrile; at 20 ℃; for 29h;

Reference yield:

: 6919-61-5
N-methoxy-N-methylbenzamide

: 1192573-82-2
2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 20 °C

1.2: 0 - 20 °C

2.1: pyridine; hydroxylamine hydrochloride / 75 h / 20 - 50 °C

3.1: caesium carbonate / potassium iodide / acetonitrile / 29 h / 20 °C

With pyridine; ethylmagnesium bromide; hydroxylamine hydrochloride; caesium carbonate; potassium iodide; In diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: (1-methyl-1H-imidazol-5-yl)(phenyl)methanone

: 1192573-82-2
2-{6-[({[(1-methyl-1H-imidazol-5-yl)(phenyl)methylene]amino}oxy)methyl]pyridin-2-yl}-1H-isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydroxylamine hydrochloride / 75 h / 20 - 50 °C

2: caesium carbonate / potassium iodide / acetonitrile / 29 h / 20 °C

With pyridine; hydroxylamine hydrochloride; caesium carbonate; potassium iodide; In acetonitrile;