2-methylene-8-phenoxyoctanoic acid

Base Information

Chemical Name:2-methylene-8-phenoxyoctanoic acid
CAS No.:220077-61-2
Molecular Formula:C₁₅H₂₀O₃
Molecular Weight:248.322
Hs Code.:

Synonyms:2-methylene-8-phenoxyoctanoic acid

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Chemical Property of 2-methylene-8-phenoxyoctanoic acid

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Technology Process of 2-methylene-8-phenoxyoctanoic acid

There total 1 articles about 2-methylene-8-phenoxyoctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.9%

: 220077-60-1
ethyl 2-methylene-8-phenoxyoctanoate

: 220077-61-2
2-methylene-8-phenoxyoctanoic acid

Guidance literature:: With potassium hydroxide; In ethanol; at 25 ℃; for 8h;
DOI:10.1016/S0968-0896(98)00175-8

Reference yield: 93.8%

: 220077-61-2
2-methylene-8-phenoxyoctanoic acid

: 220077-62-3
2-methylene-8-(2,4-dinitrophenoxy)octanoic acid

Guidance literature:: With nitronium tetrafluoborate; In dichloromethane; for 0.5h;
DOI:10.1016/S0968-0896(98)00175-8

Reference yield:

: 220077-61-2
2-methylene-8-phenoxyoctanoic acid

: 2-<6-(2,4-dinitrophenoxy)hexyl>oxiranecarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93.8 percent / NO₂BF₄ / CH₂Cl₂ / 0.5 h

2: 74.3 percent / DBU / benzene / 1 h / 25 °C

3: 96 percent / MCPBA, 3-tert-butyl-4-hydroxy-5-methylphenylsulfide / 1,2-dichloro-ethane / 14 h / 60 °C

4: 74 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

With nitronium tetrafluoborate; 3-methyl-4-hydroxy-5-tert-butylbenzenethiol; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; benzene;
DOI:10.1016/S0968-0896(98)00175-8