Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

Base Information

Chemical Name:Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;
CAS No.:89478-44-4
Molecular Formula:CF₃O₃S*C₂₇H₂₅N₂O₂
Molecular Weight:558.578
Hs Code.:

Synonyms:Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

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Chemical Property of Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

Chemical Property:

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Technology Process of Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

There total 1 articles about Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 5407-87-4
2-Amino-4,6-dimethylpyridine

: 85056-65-1
2-(ethoxycarbonyl)-4,6-diphenylpyrylium trifluoromethanesulphonate

: 89478-44-4
Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

Guidance literature:: In dichloromethane; at 25 ℃; for 12h;
DOI:10.1039/P19830002623

Reference yield:

: 89478-44-4
Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

: 19625-63-9
2,4-diphenylpicolinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. sodium hydroxide, 2.) hydrochloric acid (pH 2) / 1.) 25 deg C, 48 h, 2.) 0 deg C --> 25 deg C, 2 h

2: aq. sodium hydroxide / aq. ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol;
DOI:10.1039/P19830002623

Reference yield:

: 89478-44-4
Trifluoro-methanesulfonate2-ethoxycarbonyl-4',6'-dimethyl-4,6-diphenyl-[1,2']bipyridinyl-1-ylium;

: 16115-08-5
4,6-dimethyl-2-pyridone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. sodium hydroxide, 2.) hydrochloric acid (pH 2) / 1.) 25 deg C, 48 h, 2.) 0 deg C --> 25 deg C, 2 h

2: 60 percent / aq. sodium hydroxide / aq. ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol;
DOI:10.1039/P19830002623