C₄₈H₃₁N₃

Base Information

Chemical Name:C₄₈H₃₁N₃
CAS No.:1448304-58-2
Molecular Formula:C₄₈H₃₁N₃
Molecular Weight:649.794
Hs Code.:

C<sub>48</sub>H<sub>31</sub>N<sub>3</sub>

Synonyms:C₄₈H₃₁N₃

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Chemical Property of C₄₈H₃₁N₃

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Technology Process of C₄₈H₃₁N₃

There total 4 articles about C₄₈H₃₁N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1448304-58-2
C₄₈H₃₁N₃

Guidance literature:: With tri-tert-butyl phosphine; potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 12h; Reflux; Inert atmosphere;

Reference yield: 72.0%

: 591-50-4
iodobenzene

: C₄₂H₂₇N₃

: 1448304-58-2
C₄₈H₃₁N₃

Guidance literature:: With tri-tert-butyl phosphine; sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; toluene; for 12h; Inert atmosphere; Reflux;

Reference yield:

: 855738-89-5
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- 9H-carbazole

: 1448304-58-2
C₄₈H₃₁N₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane; water / 16 h / 90 °C / Inert atmosphere

2: triethyl phosphite / 12 h / 160 °C / Inert atmosphere

3: potassium carbonate; 1,10-Phenanthroline; copper(l) iodide / N,N-dimethyl-formamide / 24 h / Inert atmosphere; Reflux

4: sodium t-butanolate; tri-tert-butyl phosphine / 5,5-dimethyl-1,3-cyclohexadiene; toluene / 12 h / Inert atmosphere; Reflux

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,10-Phenanthroline; tri-tert-butyl phosphine; potassium carbonate; sodium t-butanolate; triethyl phosphite; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide; toluene;