Technology Process of C29H36N6O4
There total 7 articles about C29H36N6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane; chlorotriisopropylsilane;
at 20 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C
2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 15 h / 20 °C
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 70 °C
5.1: trifluoroacetic acid / dichloromethane; chlorotriisopropylsilane / 6 h / 20 °C
With
potassium carbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
dichloromethane; chlorotriisopropylsilane; N,N-dimethyl-formamide; tert-butyl alcohol;
1.1: Buchwald-Hartwig Pd catalyzed aryl C-N formation;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogen / platinum on carbon / thiophene; methanol; di-isopropyl ether / 16 h
2.1: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C
3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 15 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C
5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 70 °C
6.1: trifluoroacetic acid / dichloromethane; chlorotriisopropylsilane / 6 h / 20 °C
With
hydrogen; potassium carbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; XPhos;
tris-(dibenzylideneacetone)dipalladium(0); platinum on carbon;
In
thiophene; methanol; dichloromethane; di-isopropyl ether; chlorotriisopropylsilane; N,N-dimethyl-formamide; tert-butyl alcohol;
2.1: Buchwald-Hartwig Pd catalyzed aryl C-N formation;