N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide

Base Information

• Chemical Name: N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide
• CAS No.: 288099-60-5
• Molecular Formula: C₅₈H₆₄N₁₀O₁₂S₈
• Molecular Weight: 1349.73

Synonyms:N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide

Chemical Property of N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide

Chemical Property:

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Technology Process of N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide

There total 2 articles about N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.8%

(2-methoxy-1,3-phenylene)bis[(2-thioxothiazolidin-3-yl)methanone] + N,N,N',N'-tetrakis-(2-aminoethyl)ethylenediamine (4097-90-9) → N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide (288099-60-5)

Guidance literature:

In dichloromethane; for 24h;

DOI:10.1021/ja064902x

Reference yield: 33.0%

(2-methoxy-1,3-phenylene)bis[(2-thioxothiazolidin-3-yl)methanone] + N1,N1'-(ethane-1,2-diyl)bis(N1-(2-aminoethyl)ethane-1,2-diamine) tetrahydrobromide → N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide (288099-60-5)

Guidance literature:

With trimethylamine; In dichloromethane; N,N-dimethyl acetamide; dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

Reference yield: 72.0%

N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]-N,N',N'',N'''-[1,2-ethanediylbis(nitrilodi-2,1-ethanediyl)]tetrakis[2-methoxy-3-[(2-thioxo-3-thiazolidinyl)carbonyl]]benzamide (288099-60-5) + (R)-1-phenyl-ethyl-amine (3886-69-9) → C78H88N10O12

Guidance literature:

In dichloromethane; for 24h;

DOI:10.1021/ja064902x

upstream raw materials:

N,N,N',N'-tetrakis-(2-aminoethyl)ethylenediamine

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