C₂₇H₃₃NO₂Si

Base Information

• Chemical Name: C₂₇H₃₃NO₂Si
• CAS No.: 160724-95-8
• Molecular Formula: C₂₇H₃₃NO₂Si
• Molecular Weight: 431.65
• Mol file: 160724-95-8.mol

Synonyms:C₂₇H₃₃NO₂Si

Chemical Property of C₂₇H₃₃NO₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₇H₃₃NO₂Si

There total 1 articles about C₂₇H₃₃NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-(trimethylsilyl)but-3-yn-1-ol (2117-12-6) + C20H21NO2 (160724-73-2) → C27H33NO2Si (160724-95-8)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 12h; Ambient temperature;

Reference yield:

C27H33NO2Si (160724-95-8) → C27H35NO2Si

Guidance literature:

Multi-step reaction with 3 steps

2: 53 percent / AIBN, Bu₃SnH / benzene / 22 h / Heating

3: 92 percent / m-CPBA / CH₂Cl₂ / 2 h / Ambient temperature

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

Reference yield:

C27H33NO2Si (160724-95-8) → C24H27NO2

Guidance literature:

Multi-step reaction with 4 steps

2: 53 percent / AIBN, Bu₃SnH / benzene / 22 h / Heating

3: 92 percent / m-CPBA / CH₂Cl₂ / 2 h / Ambient temperature

4: 13 percent / 90percent HCOOH / 0.25 h / Heating

With formic acid; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

upstream raw materials:

4-(trimethylsilyl)but-3-yn-1-ol

C₂₀H₂₁NO₂

Downstream raw materials:

C₃₃H₃₉NOSSi

7α-formyl-1,2-dehydropyrrolizidone

C₂₇H₃₅NOSi

C₂₄H₂₇NO₂

Refernces