isophthalonitrile oxide

Base Information

Chemical Name:isophthalonitrile oxide
CAS No.:18660-06-5
Molecular Formula:C₈H₄N₂O
Molecular Weight:144.133
Hs Code.:

Synonyms:isophthalonitrile oxide

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Chemical Property of isophthalonitrile oxide

Chemical Property:

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Technology Process of isophthalonitrile oxide

There total 4 articles about isophthalonitrile oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20680-35-7
3-cyanophenylhydroximic acid chloride

: 18660-06-5
isophthalonitrile oxide

Guidance literature:: With potassium carbonate; In water;
DOI:10.1016/j.bmcl.2021.127979

Reference yield:

: 64847-76-3
3-(hydroxyimino)methylbenzonitrile

: 18660-06-5
isophthalonitrile oxide

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 3.33 h / 20 - 35 °C

2: potassium carbonate / water

With N-chloro-succinimide; potassium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2021.127979

Reference yield:

: 24964-64-5
3-Cyanobenzaldehyde

: 18660-06-5
isophthalonitrile oxide

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; sodium hydrogencarbonate / ethanol / 2 h / 50 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 3.33 h / 20 - 35 °C

3: potassium carbonate / water

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium hydrogencarbonate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2021.127979