(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

Base Information

Chemical Name:(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone
CAS No.:157068-43-4
Molecular Formula:C₁₆H₁₅ClN₂O₃S
Molecular Weight:350.826
Hs Code.:

Synonyms:(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

Suppliers and Price of (E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

Chemical Property:

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Technology Process of (E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

There total 1 articles about (E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61341-26-2
3-methylthenoyl chloride

: 89-59-8
4-chloro-2-nitrotoluene

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 157068-43-4
(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

Guidance literature:: With triethylamine; Yield given. Multistep reaction; 1.) DMF;
DOI:10.1021/jm00045a004

Reference yield: 61.0%

: 157068-43-4
(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

: 157068-46-7
2-(4-chloro-2-nitrophenyl)-1-(3-methyl-thien-2-yl)ethanone

Guidance literature:: With water; In 1,4-dioxane; Heating;
DOI:10.1021/jm00045a004

Reference yield:

: 157068-43-4
(E)-2-(4-Chloro-2-nitro-phenyl)-3-dimethylamino-1-(3-methyl-thiophen-2-yl)-propenone

: 1027308-60-6
4-chloro-N-methyl-α-(3-methyl-thien-2-yl)-2-nitrobenzeneethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / H₂O / dioxane / Heating

2: NaBH₃CN

With water; sodium cyanoborohydride; In 1,4-dioxane;
DOI:10.1021/jm00045a004