Technology Process of C29H42O5
There total 4 articles about C29H42O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C30H44O5;
With
lithium hydroxide;
In
methanol; water;
at 65 ℃;
for 0.75h;
Inert atmosphere;
With
acetic acid;
In
methanol; water;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ol200099n
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / methanol; dichloromethane / Inert atmosphere
2.1: lithium hydroxide / methanol; water / 0.75 h / 65 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
potassium carbonate; lithium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1021/ol200099n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium osmate(VI) dihydrate; potassium hexacyanoferrate (III); C65H83N6O4(1+)*I(1-); methanesulfonamide; potassium carbonate / water; tert-butyl alcohol / 19 h / 0 °C / Inert atmosphere
2.1: pyridine / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere
3.1: potassium carbonate / methanol; dichloromethane / Inert atmosphere
4.1: lithium hydroxide / methanol; water / 0.75 h / 65 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
With
pyridine; potassium osmate(VI) dihydrate; potassium hexacyanoferrate (III); methanesulfonamide; C65H83N6O4(1+)*I(1-); potassium carbonate; lithium hydroxide;
In
methanol; dichloromethane; water; tert-butyl alcohol;
1.1: Sharpless dihydroxylation;
DOI:10.1021/ol200099n
