1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

Base Information

Chemical Name:1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside
CAS No.:84309-67-1
Molecular Formula:C₁₇H₂₂O₃
Molecular Weight:274.36
Hs Code.:

Synonyms:1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

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Chemical Property of 1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

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Technology Process of 1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

There total 7 articles about 1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 84283-98-7,84284-00-4
methyl 6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-α-D-talopyranoside

: 84309-67-1
1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

Guidance literature:: With sulfuric acid; In 1,4-dioxane; for 3h; Ambient temperature;
DOI:10.1016/S0008-6215(00)81888-1

Reference yield:

: 100-44-7
benzyl chloride

: 84309-67-1
1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 49.2 percent / sodium hydride / dimethylformamide / 3 h / Ambient temperature

2: 0.048 g / 12 h / Heating

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)81888-1

Reference yield:

: 84283-95-4,84283-96-5
Acetic acid (2S,4R)-2-methoxy-1-methyl-5-oxo-3-oxa-bicyclo[4.2.0]oct-4-ylmethyl ester

: 84309-67-1
1,4-anhydro-6-O-benzyl-2,3-dideoxy-2,3-C-ethylene-2,4-di-C-methyl-β-D-talopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 51.1 percent / diethyl ether / 2.5 h / 0 °C

2: sodium hydride / dimethylformamide / 3 h / Ambient temperature

3: 0.048 g / 12 h / Heating

With sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)81888-1