[η5-PhCH=C(Me)C5H4]4Cr4Se4

Base Information

Chemical Name:[η5-PhCH=C(Me)C5H4]4Cr4Se4
CAS No.:675820-07-2
Molecular Formula:C₅₆H₅₂Cr₄Se₄
Molecular Weight:1248.85
Hs Code.:

Synonyms:[η5-PhCH=C(Me)C5H4]4Cr4Se4

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Chemical Property of [η5-PhCH=C(Me)C5H4]4Cr4Se4

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Technology Process of [η5-PhCH=C(Me)C5H4]4Cr4Se4

There total 1 articles about [η5-PhCH=C(Me)C5H4]4Cr4Se4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 675820-00-5
[η5-MeC(O)C5H4]4Cr4Se4

: 1449-46-3
benzyltriphenylphosphonium bromide

: 675820-07-2
[η5-PhCH=C(Me)C5H4]4Cr4Se4

Guidance literature:: With NaOH; In methanol; chloroform; under N2 atm. mixt. (η5-MeC(O)C5H4)4Cr4Se4, Ph3PCH2PhBr, CHCl3, and NaOH in MeOH was refluxed for 1 h; react. mixt. was cooled to room temp., water was added, org. layer was dried over Na2SO4, concd., and subjected to TLC (acetone-petroleum ether-CH2Cl2 1:2:3); elem. anal.;
DOI:10.1021/om034283q