C₅₄H₅₆N₄O₁₆S₂

Base Information

Chemical Name:C₅₄H₅₆N₄O₁₆S₂
CAS No.:1262795-81-2
Molecular Formula:C₅₄H₅₆N₄O₁₆S₂
Molecular Weight:1081.19
Hs Code.:

C<sub>54</sub>H<sub>56</sub>N<sub>4</sub>O<sub>16</sub>S<sub>2</sub>

Synonyms:C₅₄H₅₆N₄O₁₆S₂

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Chemical Property of C₅₄H₅₆N₄O₁₆S₂

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Technology Process of C₅₄H₅₆N₄O₁₆S₂

There total 11 articles about C₅₄H₅₆N₄O₁₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1262795-74-3
C₂₇H₂₈N₂O₈S

: 1262795-81-2
C₅₄H₅₆N₄O₁₆S₂

Guidance literature:: With palladium(II) acetate; triphenylphosphine; In benzene; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1071/CH10359

Reference yield:

: 1262795-72-1
C₂₄H₂₆N₂O₈S

: 1262795-81-2
C₅₄H₅₆N₄O₁₆S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 18 °C / Inert atmosphere

2.1: palladium(II) acetate; triphenylphosphine / benzene / 2 h / 80 °C / Inert atmosphere

With palladium(II) acetate; sodium hydride; triphenylphosphine; In N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1071/CH10359

Reference yield:

: C₁₂H₁₆BrNO₃

: 1262795-81-2
C₅₄H₅₆N₄O₁₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,4-dioxane / 24 h / 105 °C

2.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 2 h / 18 °C / Inert atmosphere

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / tetrahydrofuran; water / 1.5 h / 90 °C / Inert atmosphere; Microwave irradiation

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 - 18 °C / Inert atmosphere

6.1: palladium(II) acetate; triphenylphosphine / benzene / 2 h / 80 °C / Inert atmosphere

With 2,6-dimethylpyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; trimethylsilyl trifluoromethanesulfonate; palladium(II) acetate; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene; 4.1: Suzuki coupling;
DOI:10.1071/CH10359