3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Base Information

Chemical Name:3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene
CAS No.:157429-93-1
Molecular Formula:C₂₉H₂₆ClN₅O₂
Molecular Weight:512.011
Hs Code.:

3'-Chloro-2',3'-dodeoxy-N<sub>6</sub>-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Synonyms:3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Suppliers and Price of 3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

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Chemical Property of 3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Chemical Property:

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Technology Process of 3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

There total 4 articles about 3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 157429-90-8
3'-Chloro-2',3'-dideoxy-5'-O,N₆-bis(triphenylmethyl)-2',3'-secoadenosin-1'-ene

: 157429-93-1
3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Guidance literature:: With zinc dibromide; In dichloromethane; Ambient temperature; 1-6 h;
DOI:10.1002/hlca.19950780714

Reference yield:

: 135216-47-6
5'-O,N⁶-bis(triphenylmethyl)-2',3'-secoadenosine

: 157429-93-1
3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / pyridine / Ambient temperature

2: 84 percent / KO(t-Bu) / tetrahydrofuran / 75 h / 40 °C

3: 85 percent / LiCl / dimethylformamide / 25 h / 85 °C

4: 70 percent / ZnBr₂ / CH₂Cl₂ / Ambient temperature; 1-6 h

With potassium tert-butylate; lithium chloride; zinc dibromide; In tetrahydrofuran; pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19950780714

Reference yield:

: 157429-88-4
2'-Deoxy-3'-O-<(tol-4-yl)sulfonyl>-5'-O,N6-bis(triphenylmethyl)-2',3'-secoadenosin-1'-ene

: 157429-93-1
3'-Chloro-2',3'-dodeoxy-N₆-(triphenylmethyl)-2',3'-secoadenosin-1'-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LiCl / dimethylformamide / 25 h / 85 °C

2: 70 percent / ZnBr₂ / CH₂Cl₂ / Ambient temperature; 1-6 h

With lithium chloride; zinc dibromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19950780714