(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

Base Information

Chemical Name:(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene
CAS No.:1415757-69-5
Molecular Formula:C₅₆H₃₆N₄
Molecular Weight:764.929
Hs Code.:

Synonyms:(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

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Chemical Property of (E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

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Technology Process of (E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

There total 4 articles about (E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 84907-53-9
(E)-1,2-bis-(p-phenylaldehyde)ethene

: 62-53-3
aniline

: 84-11-7
9,10-phenanthrenequinone

: 1415757-69-5
(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

Guidance literature:: With ammonium acetate; In acetic acid; at 140 ℃; for 48h; Inert atmosphere;
DOI:10.1002/adma.201202222

Reference yield:

: 18869-30-2
(E)-4,4'-dibromostilbene

: 1415757-69-5
(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C / Inert atmosphere

1.2: 8 h / -78 - 20 °C

2.1: acetic acid; ammonium acetate / 48 h / 140 °C / Sealed tube

With n-butyllithium; ammonium acetate; acetic acid; In tetrahydrofuran; hexane;

Reference yield:

: 589-15-1
1-bromomethyl-4-bromobenzene

: 1415757-69-5
(E)-1,2-bis(4-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)phenyl)ethene

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 12 h / 150 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / Inert atmosphere; Cooling with ice

3.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C / Inert atmosphere

3.2: 8 h / -78 - 20 °C

4.1: acetic acid; ammonium acetate / 48 h / 140 °C / Sealed tube

With n-butyllithium; potassium tert-butylate; ammonium acetate; acetic acid; In tetrahydrofuran; hexane; toluene; 1.1: |Michaelis-Arbuzov Synthesis / 2.1: |Horner-Wadsworth-Emmons Olefination;