2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

Base Information

Chemical Name:2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid
CAS No.:85466-33-7
Molecular Formula:C₁₈H₂₇NO₅S
Molecular Weight:369.482
Hs Code.:

Synonyms:2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

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Chemical Property of 2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

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Technology Process of 2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

There total 2 articles about 2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 53599-14-7
2-amino-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

: 85466-33-7
2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 15h; Cooling with ice;

Reference yield:

: 158944-97-9
2-(tert-butoxycarbonylamino)-3-mercapto-3-methylbutanoic acid

: 85466-33-7
2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

Guidance literature:: With sodium hydroxide;
DOI:10.1016/j.bmcl.2005.08.050

Reference yield:

: 85466-33-7
2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)thio)-3-methylbutanoic acid

: 616-34-2
methoxycarbonylmethylamine

: C₂₁H₃₂N₂O₆S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;