Technology Process of C29H36N2O4S2
There total 4 articles about C29H36N2O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-methyl-N-(2-propenyl)benzenesulfonamide;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
for 0.5h;
C20H27NO5S2;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 14h;
DOI:10.1002/asia.201200201
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C
2.1: triethylamine / dichloromethane / 1 h / 0 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C
3.2: 14 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; sodium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/asia.201200201
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 45 h / 0 - 20 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C
3.1: triethylamine / dichloromethane / 1 h / 0 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C
4.2: 14 h / 0 - 20 °C
With
di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/asia.201200201
