2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

Base Information

Chemical Name:2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia
CAS No.:82749-86-8
Molecular Formula:C₁₉H₁₈N₂O₆S₂*H₃N
Molecular Weight:451.524
Hs Code.:

Synonyms:2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

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Chemical Property of 2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

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Technology Process of 2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

There total 6 articles about 2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82749-87-9
2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid phenyl ester

: 82749-86-8
2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

Guidance literature:: With ammonium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; under 75.006 Torr;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 82749-86-8
2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 50 percent / butan-2-one / 6 h / Heating

3: propan-2-ol / 10 h / Heating

4: H₂, aq. NH₃ / 10percent Pd/C / tetrahydrofuran / 20 °C / 75.01 Torr

With ammonium hydroxide; ammonia; hydrogen; palladium on activated charcoal; In tetrahydrofuran; isopropyl alcohol; butanone;
DOI:10.1021/jm00362a017

Reference yield:

: 100-67-4
potassium phenolate

: 82749-86-8
2-Benzylamino-4-phenoxy-5-sulfamoyl-benzenesulfonic acid; compound with ammonia

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / butan-2-one / 6 h / Heating

2: propan-2-ol / 10 h / Heating

3: H₂, aq. NH₃ / 10percent Pd/C / tetrahydrofuran / 20 °C / 75.01 Torr

With ammonium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; isopropyl alcohol; butanone;
DOI:10.1021/jm00362a017