5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

Base Information

Chemical Name:5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole
CAS No.:318467-53-7
Molecular Formula:C₂₃H₂₇N₅OS₂
Molecular Weight:453.632
Hs Code.:

5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4<i>H</i>-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

Synonyms:5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

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Chemical Property of 5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

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Technology Process of 5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

There total 3 articles about 5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 824-94-2
p-methoxybenzyl chloride

: 318467-39-9
4-adamantan-1-yl-5-(4-methyl-[1,2,3]thiadiazol-5-yl)-2,4-dihydro-[1,2,4]triazole-3-thione

: 318467-53-7
5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

Guidance literature:: 4-adamantan-1-yl-5-(4-methyl-[1,2,3]thiadiazol-5-yl)-2,4-dihydro-[1,2,4]triazole-3-thione; With potassium hydroxide; In ethanol; for 0.5h;

p-methoxybenzyl chloride; In ethanol; at 20 ℃; for 18h;
DOI:10.1002/1521-4184(200010)333:10<347::AID-ARDP347>3.0.CO;2-6

Reference yield:

: 4411-26-1
1-adamantylisothiocyanate

: 318467-53-7
5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / aq. NaOH / ethanol / 24 h

2.1: 55 percent / NaHCO₃ / H₂O; dimethylformamide / 4 h / 140 °C

3.1: KOH / ethanol / 0.5 h

3.2: 86 percent / ethanol / 18 h / 20 °C

With potassium hydroxide; sodium hydroxide; sodium hydrogencarbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/1521-4184(200010)333:10<347::AID-ARDP347>3.0.CO;2-6

Reference yield:

: 318467-33-3
C₁₅H₂₁N₅OS₂

: 318467-53-7
5-[4-adamantan-1-yl-5-(4-methoxy-benzylsulfanyl)-4H-[1,2,4]triazol-3-yl]-4-methyl-[1,2,3]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 55 percent / NaHCO₃ / H₂O; dimethylformamide / 4 h / 140 °C

2.1: KOH / ethanol / 0.5 h

2.2: 86 percent / ethanol / 18 h / 20 °C

With potassium hydroxide; sodium hydrogencarbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/1521-4184(200010)333:10<347::AID-ARDP347>3.0.CO;2-6