H₂N-Lys(Z)-O-decyl(F₁₇)

Base Information

Chemical Name:H₂N-Lys(Z)-O-decyl(F₁₇)
CAS No.:1325213-17-9
Molecular Formula:C₂₄H₂₄F₁₇N₃O₃
Molecular Weight:725.446
Hs Code.:

H<sub>2</sub>N-Lys(Z)-O-decyl(F<sub>17</sub>)

Synonyms:H₂N-Lys(Z)-O-decyl(F₁₇)

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Chemical Property of H₂N-Lys(Z)-O-decyl(F₁₇)

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Technology Process of H₂N-Lys(Z)-O-decyl(F₁₇)

There total 3 articles about H₂N-Lys(Z)-O-decyl(F₁₇) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 688063-72-1
Boc-Lys(Z)-O-decyl(F₁₇)

: 1325213-17-9
H₂N-Lys(Z)-O-decyl(F₁₇)

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1002/ejoc.201100648

Reference yield:

: 30670-30-5
2-(perfluoro-n-octyl)ethylamine

: 1325213-17-9
H₂N-Lys(Z)-O-decyl(F₁₇)

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere; Reflux

2.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 15 h / 20 °C

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/ejoc.201100648

Reference yield:

: 2389-45-9
Boc-Lys(Z)-OH

: 1325213-17-9
H₂N-Lys(Z)-O-decyl(F₁₇)

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere; Reflux

2.1: methoxybenzene; trifluoroacetic acid / dichloromethane / 15 h / 20 °C

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/ejoc.201100648