4-formyl-4'-dodecyloxybiphenyl

Base Information

Chemical Name:4-formyl-4'-dodecyloxybiphenyl
CAS No.:121118-80-7
Molecular Formula:C₂₅H₃₄O₂
Molecular Weight:366.544
Hs Code.:

Synonyms:4-formyl-4'-dodecyloxybiphenyl

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Chemical Property of 4-formyl-4'-dodecyloxybiphenyl

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Technology Process of 4-formyl-4'-dodecyloxybiphenyl

There total 1 articles about 4-formyl-4'-dodecyloxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 121118-80-7
4-formyl-4'-dodecyloxybiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KOH / 1.) EtOH, reflux, 1 h, 2.) EtOH, reflux, 13 h

2: 1.) n-BuLi / 1.) benzene, hexane, RT, 30 min, 2.) benzene, hexane, RT, 2 h

With potassium hydroxide; n-butyllithium;
DOI:10.1039/a805715j

Reference yield:

: 121118-80-7
4-formyl-4'-dodecyloxybiphenyl

: 4'-dodecyloxy-biphenyl-4-carboxylic acid 2,3-bis-hydroxyamino-2,3-dimethyl-butyl ester

: 4'-dodecyloxy-biphenyl-4-carboxylic acid 2-(4'-dodecyloxy-biphenyl-4-yl)-1,3-dihydroxy-4,5,5-trimethyl-imidazolidin-4-ylmethyl ester

Guidance literature:: With toluene-4-sulfonic acid; at 25 ℃;
DOI:10.1021/jo0354443

Reference yield:

: 21211-65-4
di(pyrrol-2-yl)methane

: 121118-80-7
4-formyl-4'-dodecyloxybiphenyl

: 5,15-bis(4-dodecyloxybiphenyl)porphyrin

Guidance literature:: With chloranil; trifluoroacetic acid; Yield given; Multistep reaction; 1.) CH₂Cl₂, RT, 15 h, 2.) CH₂Cl₂, reflux, 1 h;
DOI:10.1039/a805715j