(E)-4-fluorostyryl-2'-tributylphosphonium iodide

Base Information

• Chemical Name: (E)-4-fluorostyryl-2'-tributylphosphonium iodide
• CAS No.: 1092362-62-3
• Molecular Formula: C₂₀H₃₃FP*I
• Molecular Weight: 450.359
• Mol file: 1092362-62-3.mol

Synonyms:(E)-4-fluorostyryl-2'-tributylphosphonium iodide

Chemical Property of (E)-4-fluorostyryl-2'-tributylphosphonium iodide

Chemical Property:

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Technology Process of (E)-4-fluorostyryl-2'-tributylphosphonium iodide

There total 1 articles about (E)-4-fluorostyryl-2'-tributylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

α-trimethylsilyl(methyl)tributylphosphonium iodide (1092362-60-1) + 4-fluorobenzaldehyde (459-57-4) → (E)-4-fluorostyryl-2'-tributylphosphonium iodide (1092362-62-3)

Guidance literature:

α-trimethylsilyl(methyl)tributylphosphonium iodide; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 0.666667h; Inert atmosphere;

4-fluorobenzaldehyde; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;

DOI:10.1002/chem.200801358

upstream raw materials:

α-trimethylsilyl(methyl)tributylphosphonium iodide

4-fluorobenzaldehyde