6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

Base Information

Chemical Name:6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile
CAS No.:957114-97-5
Molecular Formula:C₁₇H₁₇ClN₂O
Molecular Weight:300.788
Hs Code.:

Synonyms:6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

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Chemical Property of 6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

Chemical Property:

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Technology Process of 6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

There total 4 articles about 6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarboxamide

: 957114-97-5
6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

Guidance literature:: 6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarboxamide; With trichlorophosphate; at 60 ℃; for 4h;

With sodium hydroxide; In water; at 0 ℃;

Reference yield:

: 892963-42-7
6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarboxylic acid

: 957114-97-5
6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2.1: ammonia / diethyl ether; water / 0.17 h

3.1: trichlorophosphate / 4 h / 60 °C

3.2: 0 °C

With oxalyl dichloride; ammonia; trichlorophosphate; N,N-dimethyl-formamide; In diethyl ether; dichloromethane; water;

Reference yield:

: 892663-68-2
ethyl 6-[{5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl]-2-pyridinecarboxylate

: 957114-97-5
6-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-2-pyridinecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; ethanol; water / 2 h / 50 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

3.1: ammonia / diethyl ether; water / 0.17 h

4.1: trichlorophosphate / 4 h / 60 °C

4.2: 0 °C

With sodium hydroxide; oxalyl dichloride; ethanol; ammonia; water; trichlorophosphate; N,N-dimethyl-formamide; In diethyl ether; dichloromethane; water;