C₁₀H₁₃BrO₂

Base Information

• Chemical Name: C₁₀H₁₃BrO₂
• CAS No.: 1301147-34-1
• Molecular Formula: C₁₀H₁₃BrO₂
• Molecular Weight: 245.116
• Hs Code.: 2909309090
• Mol file: 1301147-34-1.mol

Synonyms:C₁₀H₁₃BrO₂

Chemical Property of C₁₀H₁₃BrO₂

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-6-(methoxymethoxy)-o-xylene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₃BrO₂

There total 1 articles about C₁₀H₁₃BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-bromo-2,3-dimethylphenol (22802-37-5) + chloromethyl methyl ether (107-30-2) → C10H13BrO2 (1301147-34-1)

Guidance literature:

4-bromo-2,3-dimethylphenol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 23 ℃; for 0.833333h; Inert atmosphere;

chloromethyl methyl ether; In tetrahydrofuran; mineral oil; at 23 ℃; for 2.16667h; Inert atmosphere;

DOI:10.1002/anie.201102688

Reference yield: 65.0%

carbon dioxide (124-38-9,18923-20-1) + C10H13BrO2 (1301147-34-1) → C11H14O4 (1333231-02-9)

Guidance literature:

C₁₀H₁₃BrO₂; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

carbon dioxide; In tetrahydrofuran; at 23 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201102688

Reference yield:

C10H13BrO2 (1301147-34-1) → methyl 2,3-dimethyl-4-hydroxybenzene-1-carboxylate (5628-56-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.5 h / 23 °C / Inert atmosphere

2.1: sulfuric acid / 13 h / Inert atmosphere; Reflux

With n-butyllithium; sulfuric acid; In tetrahydrofuran;

DOI:10.1002/anie.201102688

upstream raw materials:

4-bromo-2,3-dimethylphenol

chloromethyl methyl ether

Downstream raw materials:

χ,χ-caroten-18,18-dioic acid

dimethyl (1E,3E,5E,7E,9E,11E,13E,15E,17E) 4,4'-(3,7,12,16-tetramethyloctadeca-1,3,5,7,9,11,13,15,17-nonaene-1,18-diyl)-bis-(2,3-dimethylbenzoate)

C₄₀H₄₆O₄

C₁₁H₁₁F₃O₅S