tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate

Base Information

• Chemical Name: tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate
• CAS No.: 1097639-65-0
• Molecular Formula: C₁₉H₂₇N₅O₅
• Molecular Weight: 405.454

Synonyms:tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate

Chemical Property of tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate

There total 2 articles about tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 1-[3-(methylsulfonyl)-1,2,4-triazin-6-yl]ethylcarbamate + 3,4,5-Trimethoxyaniline (24313-88-0) → tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate (1097639-65-0)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; for 24h;

Reference yield:

C11H18N4O3S + 3,4,5-Trimethoxyaniline (24313-88-0) → tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate (1097639-65-0)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2008.09.100

Reference yield:

tert-butyl 1-{3-[(3,4,5-trimethoxyphenyl)amino]-1,2,4-triazin-6-yl}ethylcarbamate (1097639-65-0) → 6-(1-aminoethyl)-N-(3,4,5-trimethoxyphenyl)-1,2,4-triazin-3-amine hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; for 0.5h;

upstream raw materials:

3,4,5-Trimethoxyaniline

Downstream raw materials:

6-(1-aminoethyl)-N-(3,4,5-trimethoxyphenyl)-1,2,4-triazin-3-amine

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