tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat

Base Information

• Chemical Name: tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat
• CAS No.: 47594-84-3
• Molecular Formula: C₁₈H₂₆N₄O₆
• Molecular Weight: 394.428
• Mol file: 47594-84-3.mol

Synonyms:tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat

Chemical Property of tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat

There total 2 articles about tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butoxycarbonyl)-β-tert-butyl-L-aspartic acid p-nitrophenyl ester (29365-05-7) → tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat (47594-84-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / Ambient temperature

2: CF₃CO₂H / Ambient temperature

With triethylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;

DOI:10.1021/ja01019a037

Reference yield:

(S)-N-[2-(N'-Benzyloxycarbonyl-hydrazino)-2-oxo-ethyl]-3-tert-butoxycarbonylamino-succinamic acid tert-butyl ester (19636-07-8) → tert.-Butyl-L-asparagyl-glycyl-benzyloxycarbonyl-hydrazid-trifluoroacetat (47594-84-3)

Guidance literature:

With trifluoroacetic acid; Ambient temperature;

DOI:10.1021/ja01019a037

upstream raw materials:

(S)-N-[2-(N'-Benzyloxycarbonyl-hydrazino)-2-oxo-ethyl]-3-tert-butoxycarbonylamino-succinamic acid tert-butyl ester

N-(tert-butoxycarbonyl)-β-tert-butyl-L-aspartic acid p-nitrophenyl ester