2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

Base Information

Chemical Name:2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)
CAS No.:1307298-00-5
Molecular Formula:C₁₆H₁₄Br₄O₂S₂
Molecular Weight:622.034
Hs Code.:

Synonyms:2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

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Technology Process of 2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

There total 1 articles about 2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2-(bromomethyl)-4,6-dibromophenol: 4186-54-3
2-(bromomethyl)-4,6-dibromophenol

: 540-63-6
ethane-1,2-dithiol

: 1307298-00-5
2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 24h; Darkness;
DOI:10.1016/j.jorganchem.2011.01.021

Reference yield: 89.0%

: 1307298-00-5
2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

: 24356-01-2
tetrabenzylzirconium(IV)

: (2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenolato)) dibenzylzirconium

Guidance literature:: In toluene; under N2, Schlenk techniques; soln. of diphenol ligand in toluene added dropwise to soln. of ZrBz4 in toluene, mixt. stirred at room temp. for 4h; evapn. under vac., pentane added, solid obtained after removal of pentane;
DOI:10.1016/j.jorganchem.2011.01.021

Reference yield: 89.0%

: 1307298-00-5
2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenol)

: 31406-67-4
tetra(benzyl)hafnium

: (2,2'-[ethane-1,2-diylbis(sulfanediylmethylene)]bis(4,6-dibromophenolato))dibenzylhafnium

Guidance literature:: In toluene; under N2, Schlenk techniques; soln. of diphenol ligand in toluene added dropwise to soln. of HfBz4 in toluene, mixt. stirred at room temp. for 3h; evapn. under vac., pentane added, solid obtained after removal of pentane;
DOI:10.1016/j.jorganchem.2011.01.021