N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

Base Information

Chemical Name:N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide
CAS No.:1565836-02-3
Molecular Formula:C₅₇H₆₆N₈O₇S
Molecular Weight:1007.27
Hs Code.:

N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

Synonyms:N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

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Chemical Property of N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

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Technology Process of N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

There total 17 articles about N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 194920-43-9,945462-84-0
biotin-PEG-NH₂·TFA

: 1440755-24-7
4-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-3-(2-phenyl-1H-benzo[d]imidazol-1-yl)butanoic acid

: 1565836-02-3
N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield:

: C₃₇H₅₂N₆O₇S

: 10206-01-6
4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenol

: 1565836-02-3
N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

Guidance literature:: With tributylphosphine; diamide; In toluene; at 65 ℃; for 24h;
DOI:10.1021/jm500632s

Reference yield:

: 1440753-42-3
2-(4-(allyloxy)phenyl)-1-benzyl-1H-benzo[d]imidazole

: 1565836-02-3
N-(18-(4-(1-benzyl-1H-benzo[d]imidazol-2-yl)phenoxy)-15-oxo-17-(2-phenyl-1H-benzo[d]imidazol-1-yl)-4,7,10-trioxa-14-azaoctadecyl)-5-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)pentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / methanol / 20 °C

2: tributylphosphine; diamide / toluene / 24 h / 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tributylphosphine; diamide; potassium carbonate; In methanol; toluene; 2: |Mitsunobu Displacement;
DOI:10.1021/jm500632s