C₁₇H₂₃ClFNO₃

Base Information

Chemical Name:C₁₇H₂₃ClFNO₃
CAS No.:1398705-98-0
Molecular Formula:C₁₇H₂₃ClFNO₃
Molecular Weight:343.826
Hs Code.:

C<sub>17</sub>H<sub>23</sub>ClFNO<sub>3</sub>

Synonyms:C₁₇H₂₃ClFNO₃

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Chemical Property of C₁₇H₂₃ClFNO₃

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Technology Process of C₁₇H₂₃ClFNO₃

There total 4 articles about C₁₇H₂₃ClFNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177947-96-5
tert-butyl 3-formylazetidine-1-carboxylate

: 1398705-98-0
C₁₇H₂₃ClFNO₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 18 h / 0 °C / Reflux

With sodium hydride; In tetrahydrofuran; 1: |Grignard Reaction;
DOI:10.1021/jm3008294

Reference yield:

: 1398705-06-0
C₁₅H₁₉ClFNO₃

: 1398705-98-0
C₁₇H₂₃ClFNO₃

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 18h; Reflux;
DOI:10.1021/jm3008294

Reference yield:

: 142253-55-2
1-(t-butyloxycarbonyl)-azetidine-3-carboxylic acid

: 1398705-98-0
C₁₇H₂₃ClFNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 18 h / 0 °C / Reflux

With oxalyl dichloride; dimethylsulfide borane complex; sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation / 3.1: |Grignard Reaction;
DOI:10.1021/jm3008294