1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide

Base Information

• Chemical Name: 1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide
• CAS No.: 1158964-44-3
• Molecular Formula: C₆₁H₆₃NO₄Si
• Molecular Weight: 902.261
• Mol file: 1158964-44-3.mol

Synonyms:1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide

Chemical Property of 1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide

There total 1 articles about 1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,6-bis(4-tert-butylphenoxy)-9-[2-(bromide)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide + trimethylsilylacetylene (1066-54-2) → 1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide (1158964-44-3)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; triphenylphosphine; In triethylamine; toluene; at 60 ℃; for 2.5h;

DOI:10.1021/jp910705q

Reference yield: 100.0%

1,6-bis(4-tert-butylphenoxy)-9-[2-(trimethylsilyl)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide (1158964-44-3) → N-(2,5-(di-tert-butyl)phenoxy)perylene-1,6-bis(4-tert-butylphenoxy)-9-ethynyl-3,4-dicarboximide (1158964-46-5)

Guidance literature:

With methanol; potassium carbonate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/chem.200801880

upstream raw materials:

trimethylsilylacetylene

Downstream raw materials:

N-(2,5-(di-tert-butyl)phenoxy)perylene-1,6-bis(4-tert-butylphenoxy)-9-ethynyl-3,4-dicarboximide