methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate

Base Information

• Chemical Name: methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate
• CAS No.: 1002106-12-8
• Molecular Formula: C₁₇H₁₆ClFN₂O₃
• Molecular Weight: 350.777

Synonyms:methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate

Chemical Property of methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate

Chemical Property:

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Technology Process of methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate

There total 2 articles about methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-6-chloro-3-(chloro(hydroxyimino)methyl)-2-fluorobenzoate (1002106-11-7) + 4-aminoethylbenzene (589-16-2) → methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate (1002106-12-8)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

methyl-6-chloro-3-(chloro(hydroxyimino)methyl)-2-fluorobenzoate (1002106-11-7) + 4-aminoethylbenzene (589-16-2) → C17H16ClFN2O3 (1002106-12-8)

Guidance literature:

In tetrahydrofuran; at 23 ℃;

DOI:10.1016/j.bmcl.2008.07.111

Reference yield:

methyl 6-chloro-3-(N-(4-ethylphenyl)-N'-hydroxycarbamimidoyl)-2-fluorobenzoate (1002106-12-8) → methyl 6-chloro-3-(4-ethylphenylamino)benzo[d]isoxazole-7-carboxylate (1002106-13-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

upstream raw materials:

methyl-6-chloro-3-(chloro(hydroxyimino)methyl)-2-fluorobenzoate

4-aminoethylbenzene

Downstream raw materials:

methyl 6-chloro-3-(4-ethylphenylamino)benzo[d]isoxazole-7-carboxylate

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