3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

Base Information

Chemical Name:3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester
CAS No.:530113-29-2
Molecular Formula:C₄₁H₄₈I₄O₈S₂
Molecular Weight:1240.58
Hs Code.:

3-(4-<i>tert</i>-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-<i>tert</i>-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

Synonyms:3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

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Chemical Property of 3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

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Technology Process of 3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

There total 3 articles about 3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 80-05-7
BPA

: 3-(4-tert-butyl-2,6-diiodophenoxy)propane-1-sulfonyl chloride

: 530113-29-2
3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/ejoc.200390077

Reference yield:

: 75908-75-7
2,6-diiodo-4-(tert-butyl)phenol

: 530113-29-2
3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / KOtBu / 2-methyl-propan-2-ol / 1 h / 35 °C

2: 76 percent / SO₂Cl₂ / tetrahydrofuran; dimethylformamide / 3 h / 20 - 60 °C

3: 81 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

With sulfuryl dichloride; potassium tert-butylate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/ejoc.200390077

Reference yield:

: potassium 3-(4-tert-butyl-2,6-diiodophenoxy)propanesulfonate

: 530113-29-2
3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonic acid 4-(1-{4-[3-(4-tert-butyl-2,6-diiodo-phenoxy)-propane-1-sulfonyloxy]-phenyl}-1-methyl-ethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SO₂Cl₂ / tetrahydrofuran; dimethylformamide / 3 h / 20 - 60 °C

2: 81 percent / triethylamine / tetrahydrofuran / 0 - 20 °C

With sulfuryl dichloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200390077