[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

Base Information

Chemical Name:[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid
CAS No.:1312775-95-3
Molecular Formula:C₂₂H₁₆N₂O₃S
Molecular Weight:388.447
Hs Code.:

Synonyms:[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

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Chemical Property of [5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

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Technology Process of [5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

There total 3 articles about [5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1312775-96-4
2-(4-oxo-2-phenyliminothiazolidin-3-yl)acetic acid

: 66-99-9
β-naphthaldehyde

: 1312775-95-3
[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

Guidance literature:: With piperidine; In ethanol; for 6h; Microwave irradiation; Heating;
DOI:10.1016/j.ejmech.2011.03.068

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 1312775-95-3
[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / ethanol; water / 24 h / Reflux

2: triethylamine / ethanol / 24 h / Reflux

3: piperidine / ethanol / 6 h / Microwave irradiation; Heating

With piperidine; potassium carbonate; triethylamine; In ethanol; water; 3: Knoevenagel condensation;
DOI:10.1016/j.ejmech.2011.03.068

Reference yield:

: 2215-20-5
2-[(phenylcarbamothioyl)amino]acetic acid

: 1312775-95-3
[5-(naphthalen-2-ylmethylidene)-4-oxo-2-phenyliminothiazolidin-3-yl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 24 h / Reflux

2: piperidine / ethanol / 6 h / Microwave irradiation; Heating

With piperidine; triethylamine; In ethanol; 2: Knoevenagel condensation;
DOI:10.1016/j.ejmech.2011.03.068