benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

Base Information

Chemical Name:benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate
CAS No.:1428479-72-4
Molecular Formula:C₃₁H₃₀FN₇O₃
Molecular Weight:567.623
Hs Code.:

Synonyms:benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

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Chemical Property of benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

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Technology Process of benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

There total 1 articles about benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 462068-57-1
2-[4-(1H-1,2,3,4-tetrazol-1-ol)phenyl]acetic acid

: 1428479-07-5
4-{[(benzyloxy)carbonyl]amino}-4-[2-(3-cyano-4-fluorophenyl)ethyl]piperidinium chloride

: 1428479-72-4
benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

Guidance literature:: With pyridine; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 4h;

Reference yield:

: 1428479-72-4
benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

: 1428479-73-5
1-{4-[2-(3-cyano-4-fluorophenyl)ethyl]-4-(amino)piperidin-1-yl}-2-[4-(1H-tetrazol-1-yl)phenyl]ethanone

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol; for 2h; under 2068.65 Torr;

Reference yield:

: 1428479-72-4
benzyl {4-[2-(3-cyano-4-fluorophenyl)ethyl]-1-[4-(1H-tetrazol-1-yl)phenylacetyl]piperidin-4-yl}carbamate

: 1428478-04-9
1-{4-[2-(3-cyano-4-fluorophenyl)ethyl]-4-(dimethylamino)piperidin-1-yl}-2-[4-(1H-tetrazol-1-yl)phenyl]ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / ethanol / 2 h / 2068.65 Torr

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 16 h / 20 °C

With palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; In ethanol; 1,2-dichloro-ethane;