phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

Base Information

Chemical Name:phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate
CAS No.:157069-80-2
Molecular Formula:C₂₃H₁₈N₂O₄S
Molecular Weight:418.473
Hs Code.:

Synonyms:phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

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Chemical Property of phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

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Technology Process of phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

There total 4 articles about phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 157069-79-9
2-benzamido-4-hydroxy-3,4-dihydroisoquinolin-1(2H)-one

: 1005-56-7
phenylcarbonochloridothioate

: 157069-80-2
phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

Guidance literature:: With pyridine; In dichloromethane; at 23 ℃; for 2h;

Reference yield:

: 27326-43-8
2-vinylbenzoic acid

: 157069-80-2
phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 2 h / Heating

2: 85 percent / Et₃N / CH₂Cl₂ / 48 h / 20 °C

3: 58 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 48 h / 20 °C

4: 72 percent / pyridine / CH₂Cl₂ / 2 h / 23 °C

With pyridine; thionyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

: 28269-50-3
2-vinylbenzoic acid chloride

: 157069-80-2
phenyl 1,2,3,4-tetrahydro-1-oxo-2-benzamido-4-isoquinolinyl thiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / CH₂Cl₂ / 48 h / 20 °C

2: 58 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 48 h / 20 °C

3: 72 percent / pyridine / CH₂Cl₂ / 2 h / 23 °C

With pyridine; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;