N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

Base Information

Chemical Name:N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide
CAS No.:1245282-91-0
Molecular Formula:C₁₉H₁₄F₃NO₄
Molecular Weight:377.32
Hs Code.:

Synonyms:N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

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Chemical Property of N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

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Technology Process of N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

There total 4 articles about N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1245282-74-9
N-(3-hydroxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

: 77-78-1
dimethyl sulfate

: 1245282-91-0
N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃; for 6h;
DOI:10.1016/j.bmc.2010.06.067

Reference yield:

: 7298-67-1
5-acetamido-2-hydroxyacetophenone

: 1245282-91-0
N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / methanol / Microwave irradiation

2: dihydrogen peroxide / 24 h

With dihydrogen peroxide; lithium hydroxide; In methanol; 1: Claisen Schmidt condensation;
DOI:10.1002/mrc.2638

Reference yield:

: 454-89-7
3-Trifluoromethylbenzaldehyde

: 1245282-91-0
N-(3-methoxy-4-oxo-2-(3-(trifluoromethyl)phenyl)-4H-chromen-6-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / methanol / Microwave irradiation

2: dihydrogen peroxide / 24 h

With dihydrogen peroxide; lithium hydroxide; In methanol; 1: Claisen Schmidt condensation;
DOI:10.1002/mrc.2638