C₂₀H₃₃NO₄Si

Base Information

Chemical Name:C₂₀H₃₃NO₄Si
CAS No.:1464782-33-9
Molecular Formula:C₂₀H₃₃NO₄Si
Molecular Weight:379.572
Hs Code.:

C<sub>20</sub>H<sub>33</sub>NO<sub>4</sub>Si

Synonyms:C₂₀H₃₃NO₄Si

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Chemical Property of C₂₀H₃₃NO₄Si

Chemical Property:

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Technology Process of C₂₀H₃₃NO₄Si

There total 9 articles about C₂₀H₃₃NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1464782-13-5
C₁₃H₂₇NO₄Si

: 100-44-7
benzyl chloride

: 1464782-33-9
C₂₀H₃₃NO₄Si

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h; Inert atmosphere; Cooling with ice;
DOI:10.1039/c3cc45099f

Reference yield:

: 1251959-17-7
C₁₁H₂₁NO₄Si

: 1464782-33-9
C₂₀H₃₃NO₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 3 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h / 20 °C / 760.05 Torr / Inert atmosphere

3: diisobutylaluminium hydride / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere; Cooling with ice

With palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3cc45099f

Reference yield:

: C₁₅H₂₇NO₅Si

: 1464782-33-9
C₂₀H₃₃NO₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h / 20 °C / 760.05 Torr / Inert atmosphere

2: diisobutylaluminium hydride / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

3: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil; N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere; Cooling with ice

With palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3cc45099f