methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

Base Information

Chemical Name:methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate
CAS No.:69748-71-6
Molecular Formula:C₁₉H₃₂O₅
Molecular Weight:340.46
Hs Code.:

Synonyms:methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

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Chemical Property of methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

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Technology Process of methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

There total 7 articles about methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 69748-70-5
3-oxo-5-(2,6,6-trimethylcyclohex-1-en-1-yl)pentanal dimethyl acetal

: 96-34-4
methyl chloroacetate

: 69748-71-6
methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

Guidance literature:: With sodium methylate; In diethyl ether; at 0 ℃; for 2h;

Reference yield:

: 35031-06-2,14901-07-6
(Z)-β-ionone

: 69748-71-6
methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / H₂ / Rancy Ni / 65 °C

2: 1.58 g / MeONa / diethyl ether / 0.5 h / Ambient temperature

3: Py*HBr / 2 h / 80 °C

4: 84 percent / MeONa / diethyl ether / 2 h / 0 °C

With hydrogen; sodium methylate; Pyridine hydrobromide; nickel; In diethyl ether;

Reference yield:

: 17283-81-7
4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on

: 69748-71-6
methyl 3-<(2,2-dimethoxyethyl)-5-(2,6,6-trimethylcyclohex-1-en-1-yl)>-2,3-epoxypentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.58 g / MeONa / diethyl ether / 0.5 h / Ambient temperature

2: Py*HBr / 2 h / 80 °C

3: 84 percent / MeONa / diethyl ether / 2 h / 0 °C

With sodium methylate; Pyridine hydrobromide; In diethyl ether;