NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

Base Information

• Chemical Name: NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2
• CAS No.: 721922-86-7
• Molecular Formula: C₁₇₀H₁₉₂N₁₂Ni₃O₁₂Si₂
• Molecular Weight: 2827.71

Synonyms:NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

Chemical Property of NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

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Technology Process of NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

There total 1 articles about NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCSiMe₃)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

NiC20H8N4-5,10-(3,5-(Me2CHCH2CH2O)2C6H3)2-15,20-[CCC20H8N4BrNi-10';20'-(C6H3-3,5-(OCH2CH2CHMe2)2)2]2 (721922-85-6) + trimethylsilylacetylene (1066-54-2) → NiC20H8N4-5,10-(3,5-(Me2CHCH2CH2O)2C6H3)2-15,20-[CCC20H8N4Ni(CCSiMe3)-10',20'-(C6H3-3,5-(OCH2CH2CHMe2)2)2]2 (721922-86-7)

Guidance literature:

With Pd(PPh₃)4; CuI; In tetrahydrofuran; triethylamine; 40 equiv. of Me3SiCCH;

DOI:10.1246/cl.2004.578

Reference yield: 93.0%

NiC20H8N4-5,10-(3,5-(Me2CHCH2CH2O)2C6H3)2-15,20-[CCC20H8N4Ni(CCSiMe3)-10',20'-(C6H3-3,5-(OCH2CH2CHMe2)2)2]2 (721922-86-7) → NiC20H8N4-5,10-(3,5-(Me2CHCH2CH2O)2C6H3)2-15,20-[CCC20H8N4Ni(CCH)-10',20'-(C6H3-3,5-(OCH2CH2CHMe2)2)2]2 (721922-76-5)

Guidance literature:

With (CH₃CH₂CH₂CH₂)4NF; In dichloromethane;

DOI:10.1246/cl.2004.578

upstream raw materials:

NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄BrNi-10';20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

trimethylsilylacetylene

Downstream raw materials:

NiC₂₀H₈N₄-5,10-(3,5-(Me₂CHCH₂CH₂O)2C₆H₃)2-15,20-[CCC₂₀H₈N₄Ni(CCH)-10',20'-(C₆H₃-3,5-(OCH₂CH₂CHMe₂)2)2]2

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