C₃₁H₄₆O₆

Base Information

Chemical Name:C₃₁H₄₆O₆
CAS No.:950598-45-5
Molecular Formula:C₃₁H₄₆O₆
Molecular Weight:514.703
Hs Code.:

C<sub>31</sub>H<sub>46</sub>O<sub>6</sub>

Synonyms:C₃₁H₄₆O₆

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Chemical Property of C₃₁H₄₆O₆

Chemical Property:

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Technology Process of C₃₁H₄₆O₆

There total 26 articles about C₃₁H₄₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 950598-44-4
C₃₁H₄₅IO₆

: 950598-45-5
C₃₁H₄₆O₆

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; at 50 ℃; for 18h;
DOI:10.1021/ja073952e

Reference yield:

: 906624-11-1
(3S,6E)-8-(4-methoxybenzyloxy)-2,6-dimethylocta-1,6-dien-3-ol

: 950598-45-5
C₃₁H₄₆O₆

Guidance literature:: Multi-step reaction with 18 steps

1: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

2: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

3: DIBALH / CH₂Cl₂ / -78 °C

4: toluene / 80 °C

5: imidazole / CH₂Cl₂

6: DIBALH / CH₂Cl₂ / -78 °C

7: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

8: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

9: 63 percent / LDA / diethyl ether / -78 °C

10: imidazole / CH₂Cl₂

11: DIBALH / CH₂Cl₂ / -78 °C

12: toluene / 80 °C

13: DIBALH / CH₂Cl₂ / -78 °C

14: 97 percent / BF₃*OEt₂ / methanol / 3 h / -78 - 0 °C

15: 91 percent / PPTS / CH₂Cl₂ / 1 h / 20 °C

16: 95 percent / L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / 17 h / -40 °C

17: 93 percent / I₂; PPh₃; imidazole / CH₂Cl₂ / 3 h / 0 °C

18: 73 percent / NaBH₃CN / tetrahydrofuran / 18 h / 50 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; boron trifluoride diethyl etherate; iodine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium cyanoborohydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; lithium diisopropyl amide; 4 A molecular sieve; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 4: Wittig reaction / 7: Sharpless asymmetric epoxidation / 12: Wittig reaction / 16: Sharpless asymmetric epoxidation;
DOI:10.1021/ja073952e

Reference yield:

: 906624-08-6
(2R,3S)-2-Iodomethyl-3-[(E)-5-(4-methoxy-benzyloxy)-3-methyl-pent-3-enyl]-2-methyl-oxirane

: 950598-45-5
C₃₁H₄₆O₆

Guidance literature:: Multi-step reaction with 19 steps

1: H₂O

2: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

3: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

4: DIBALH / CH₂Cl₂ / -78 °C

5: toluene / 80 °C

6: imidazole / CH₂Cl₂

7: DIBALH / CH₂Cl₂ / -78 °C

8: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

9: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

10: 63 percent / LDA / diethyl ether / -78 °C

11: imidazole / CH₂Cl₂

12: DIBALH / CH₂Cl₂ / -78 °C

13: toluene / 80 °C

14: DIBALH / CH₂Cl₂ / -78 °C

15: 97 percent / BF₃*OEt₂ / methanol / 3 h / -78 - 0 °C

16: 91 percent / PPTS / CH₂Cl₂ / 1 h / 20 °C

17: 95 percent / L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / 17 h / -40 °C

18: 93 percent / I₂; PPh₃; imidazole / CH₂Cl₂ / 3 h / 0 °C

19: 73 percent / NaBH₃CN / tetrahydrofuran / 18 h / 50 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; boron trifluoride diethyl etherate; water; iodine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium cyanoborohydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; lithium diisopropyl amide; 4 A molecular sieve; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 5: Wittig reaction / 8: Sharpless asymmetric epoxidation / 13: Wittig reaction / 17: Sharpless asymmetric epoxidation;
DOI:10.1021/ja073952e