(2,4-dimethyl-phenyl)-glyoxylonitrile

Base Information

Chemical Name:(2,4-dimethyl-phenyl)-glyoxylonitrile
CAS No.:33108-92-8
Molecular Formula:C₁₀H₉NO
Molecular Weight:159.188
Hs Code.:

Synonyms:(2,4-dimethyl-phenyl)-glyoxylonitrile

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Chemical Property of (2,4-dimethyl-phenyl)-glyoxylonitrile

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Technology Process of (2,4-dimethyl-phenyl)-glyoxylonitrile

There total 7 articles about (2,4-dimethyl-phenyl)-glyoxylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1-(2,4-dimethylphenyl)-4,4,4-trifluoro-3,3-dihydroxy-2-(hydroxyimino)butan-1-one

: 33108-92-8
(2,4-dimethyl-phenyl)-glyoxylonitrile

Guidance literature:: With acetic anhydride; In chloroform; for 1h; Reagent/catalyst; Reflux;
DOI:10.1016/j.jfluchem.2016.04.009

Reference yield:

: 94856-20-9
1-(2,4-Dimethylphenyl)-4,4,4-trifluorobutane-1,3-dione

: 33108-92-8
(2,4-dimethyl-phenyl)-glyoxylonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium nitrite; citric acid / water / 1 h / 20 °C

2: acetic anhydride / chloroform / 1 h / Reflux

With acetic anhydride; citric acid; sodium nitrite; In chloroform; water;
DOI:10.1016/j.jfluchem.2016.04.009