C₁₆H₂₀O₃

Base Information

Chemical Name:C₁₆H₂₀O₃
CAS No.:1333080-47-9
Molecular Formula:C₁₆H₂₀O₃
Molecular Weight:260.333
Hs Code.:

C<sub>16</sub>H<sub>20</sub>O<sub>3</sub>

Synonyms:C₁₆H₂₀O₃

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Chemical Property of C₁₆H₂₀O₃

Chemical Property:

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Technology Process of C₁₆H₂₀O₃

There total 15 articles about C₁₆H₂₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72748-99-3,187035-29-6
(R)-1-Amino-2-(methoxymethyl)pyrrolidine

: 1333080-47-9
C₁₆H₂₀O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / cyclohexane / Reflux

2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 2 h / -78 °C

2.2: 2.5 h / -100 - -78 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

4.1: dipyridinium dichromate / N,N-dimethyl-formamide / 10 h / 20 °C

With dipyridinium dichromate; tetrabutyl ammonium fluoride; tert.-butyl lithium; toluene-4-sulfonic acid; In tetrahydrofuran; cyclohexane; N,N-dimethyl-formamide; pentane;
DOI:10.1016/j.tetasy.2011.06.019

Reference yield:

: 1333080-46-8
(R)-2-[4-((S)-2-hydroxy-1-methylethyl)benzyl]cyclohexanone

: 1333080-47-9
C₁₆H₂₀O₃

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; at 20 ℃; for 10h;
DOI:10.1016/j.tetasy.2011.06.019

Reference yield:

: 1333080-35-5
2-(4-((4-methoxybenzyloxy)methyl)phenyl)propan-1-ol

: 1333080-47-9
C₁₆H₂₀O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: Burkholderia cepacia lipase-PS / di-isopropyl ether / 12 h / 20 °C / Molecular sieve; Enzymatic reaction

2.1: methanol; potassium carbonate

3.1: 1H-imidazole; dmap / dichloromethane / 6 h / 0 - 20 °C

4.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C

5.1: N-Bromosuccinimide; triphenylphosphine / dichloromethane / 1 h / 0 °C

6.1: lithium diisopropyl amide / tetrahydrofuran / 2.5 h / -78 °C

6.2: 1 h / -78 °C

6.3: 0.5 h

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

8.1: dipyridinium dichromate / N,N-dimethyl-formamide / 10 h / 20 °C

With 1H-imidazole; methanol; dmap; N-Bromosuccinimide; dipyridinium dichromate; Burkholderia cepacia lipase-PS; tetrabutyl ammonium fluoride; water; potassium carbonate; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; di-isopropyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2011.06.019