2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

Base Information

Chemical Name:2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate
CAS No.:474264-53-4
Molecular Formula:C₅₉H₄₇Cl₃O₂₂
Molecular Weight:1214.37
Hs Code.:

Synonyms:2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

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Chemical Property of 2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

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Technology Process of 2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

There total 4 articles about 2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 143330-91-0
2',2',2'-trichloroethyl 3,5-dihydroxybenzoate

: 474264-52-3
3,5-bis(3',5'-dimethoxybenzoyloxy)benzoic acid

: 474264-53-4
2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

Guidance literature:: With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; at 20 ℃;
DOI:10.1021/ja020687i

Reference yield:

: 1132-21-4
3,5-dimethoxybenzoic acid

: 474264-53-4
2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DPTS; DCC / CH₂Cl₂ / 20 °C

2: 96 percent / Zn; AcOH / tetrahydrofuran / 0.25 h / 20 °C

3: 98 percent / DPTS; DCC / CH₂Cl₂ / 20 °C

With acetic acid; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja020687i

Reference yield:

: 143330-91-0
2',2',2'-trichloroethyl 3,5-dihydroxybenzoate

: 474264-53-4
2',2',2'-trichloroethyl 3,5-bis[3',5'-bis(3'',5''-dimethoxybenzoyloxy)benzoyloxy]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DPTS; DCC / CH₂Cl₂ / 20 °C

2: 96 percent / Zn; AcOH / tetrahydrofuran / 0.25 h / 20 °C

3: 98 percent / DPTS; DCC / CH₂Cl₂ / 20 °C

With acetic acid; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja020687i