N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

Base Information

Chemical Name:N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine
CAS No.:120649-87-8
Molecular Formula:C₂₉H₃₈N₇O₈P
Molecular Weight:643.637
Hs Code.:

N<sup>6</sup>-dimethylaminomethylene-5'-O-<methyl(4-phenyl-3-acetylamino-2-oxobutyl)phosphinyl>-2',3'-O-ethoxymethyleneadenosine

Synonyms:N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

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Chemical Property of N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

Chemical Property:

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Technology Process of N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

There total 5 articles about N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.1%

: 13241-24-2
2',3'-O-ethoxymethylene-N⁶-dimethylaminomethyleneadenosine

: 120649-81-2
L-(4-phenyl-3-acetylamino-2-oxobutyl)methylphosphinic acid

: 120649-87-8
N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; for 48h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89835-5

Reference yield:

: 120649-75-4
L-(4-phenyl-3-acetylamino-2-oxobutyl)methylphosphinic acid ethyl ester

: 120649-87-8
N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 96.3 percent / phosphodiesterase I / various solvent(s) / 6 h / 37 °C / pH = 8.8

2: 72.1 percent / N,N'-dicyclohexylcarbodiimide / ethyl acetate / 48 h / Ambient temperature

With dicyclohexyl-carbodiimide; phosphodiesterase I; In ethyl acetate;
DOI:10.1016/S0040-4020(01)89835-5

Reference yield:

: 4-Acetylamino-2-(ethoxy-methyl-phosphinoyl)-3-oxo-5-phenyl-pentanoic acid

: 120649-87-8
N⁶-dimethylaminomethylene-5'-O--2',3'-O-ethoxymethyleneadenosine

Guidance literature:: Multi-step reaction with 3 steps

1: 71.2 percent / aniline / xylene / Heating

2: 96.3 percent / phosphodiesterase I / various solvent(s) / 6 h / 37 °C / pH = 8.8

3: 72.1 percent / N,N'-dicyclohexylcarbodiimide / ethyl acetate / 48 h / Ambient temperature

With aniline; dicyclohexyl-carbodiimide; phosphodiesterase I; In ethyl acetate; xylene;
DOI:10.1016/S0040-4020(01)89835-5