isophthal-di-N-(4-methylphenyl)hydroxamic acid

Base Information

• Chemical Name: isophthal-di-N-(4-methylphenyl)hydroxamic acid
• CAS No.: 178690-80-7
• Molecular Formula: C₂₂H₂₀N₂O₄
• Molecular Weight: 376.412
• Mol file: 178690-80-7.mol

Synonyms:isophthal-di-N-(4-methylphenyl)hydroxamic acid

Chemical Property of isophthal-di-N-(4-methylphenyl)hydroxamic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of isophthal-di-N-(4-methylphenyl)hydroxamic acid

There total 2 articles about isophthal-di-N-(4-methylphenyl)hydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1-methyl-4-nitrobenzene (99-99-0) + N-(4-methylphenyl)hydroxylamine (623-10-9) → isophthal-di-N-(4-methylphenyl)hydroxamic acid (178690-80-7)

Guidance literature:

With pyridine; In 1,4-dioxane; at 15 ℃; for 3h;

DOI:10.1021/ja984046s

Reference yield:

N-(4-methylphenyl)hydroxylamine (623-10-9) + benzene-1,3-dicarbonyl dichloride (99-63-8) → isophthal-di-N-(4-methylphenyl)hydroxamic acid (178690-80-7)

Guidance literature:

With pyridine; In 1,4-dioxane; for 3h; Yield given; Ambient temperature;

Reference yield: 68.0%

tris(2,4-pentanedionato)gallium(III) + isophthal-di-N-(4-methylphenyl)hydroxamic acid (178690-80-7) → Ga(III)4(isophthal-di-N-(4-methylphenyl)hydroxamate)6

Guidance literature:

With triethylamine; In acetone; N2 atmosphere; addn. of Ga(acac)3 to soln. of ligand and Et3N, heating overnight, pptn.; filtration, washing (acetone), drying;

DOI:10.1021/ja984046s

upstream raw materials:

N-(4-methylphenyl)hydroxylamine

benzene-1,3-dicarbonyl dichloride

1-methyl-4-nitrobenzene