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C66H74O20

Base Information
  • Chemical Name:C66H74O20
  • CAS No.:1402736-78-0
  • Molecular Formula:C66H74O20
  • Molecular Weight:1187.3
  • Hs Code.:
C<sub>66</sub>H<sub>74</sub>O<sub>20</sub>

Synonyms:C66H74O20

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Chemical Property of C66H74O20
Chemical Property:
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Technology Process of C66H74O20

There total 3 articles about C66H74O20 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.025h;
DOI:10.1002/chem.201201624
Guidance literature:
Multi-step reaction with 3 steps
1: iodine; methyl iodide / 22 h / 115 °C
2: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; triethylamine / toluene / 18 h / 70 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.03 h / 20 °C
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; iodine; triethylamine; triphenylphosphine; methyl iodide; In tetrahydrofuran; toluene; 2: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201201624
Guidance literature:
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triphenylphosphine; triethylamine / toluene / 18 h / 70 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.03 h / 20 °C
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; In tetrahydrofuran; toluene; 1: |Sonogashira Cross-Coupling;
DOI:10.1002/chem.201201624
upstream raw materials:

C70H92N6O20

C62H72I2O20

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