tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

Base Information

Chemical Name:tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate
CAS No.:1430413-41-4
Molecular Formula:C₁₉H₃₅N₂O₆P
Molecular Weight:418.47
Hs Code.:

Synonyms:tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

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Chemical Property of tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

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Technology Process of tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

There total 4 articles about tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1430413-58-3
tert-butyl (1-cyanocyclohexyl)(3-hydroxypropyl)carbamate

: 814-49-3
diethyl chlorophosphate

: 1430413-41-4
tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

Guidance literature:: With 1-methyl-1H-imidazole; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol400788q

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 1430413-41-4
tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -40 - 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

3: 1-methyl-1H-imidazole / tetrahydrofuran / 0 °C / Inert atmosphere

With 1-methyl-1H-imidazole; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ol400788q

Reference yield:

: 1236062-60-4
C₁₆H₃₂N₂O₃Si

: 1430413-41-4
tert-butyl (1-cyanocyclohexyl)(3-((diethoxyphosphoryl)oxy)propyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide / tetrahydrofuran / -40 - 0 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

3: 1-methyl-1H-imidazole / tetrahydrofuran / 0 °C / Inert atmosphere

With 1-methyl-1H-imidazole; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ol400788q