dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]

Base Information

Chemical Name:dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]
CAS No.:1166397-92-7
Molecular Formula:C₃₄H₂₆OS₂
Molecular Weight:514.712
Hs Code.:

Synonyms:dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]

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Chemical Property of dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]

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Technology Process of dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]

There total 1 articles about dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 108143-54-0
C₁₃H₁₂N₂O

: 193087-07-9
2-(2,6-dimethylphenyl)thioxanthene-9-thione

: 1166397-92-7
dispiro[2,3-dihydro-1H-naphtho[2,1-b]pyran-1,2'-thiirane-3',9''-[2''-(2,6-dimethylphenyl)-9''H-thioxanthene]]

Guidance literature:: C₁₃H₁₂N₂O; With methanol; potassium hydroxide; magnesium sulfate; silver(l) oxide; In dichloromethane; at 0 ℃; Inert atmosphere;

2-(2,6-dimethylphenyl)thioxanthene-9-thione; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tet.2009.03.081